New macrocyclic compounds with naphthyridine units for molecular recognition studies of biotin and urea derivatives
JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY(2014)
摘要
Two macrocyclic hosts containing benzenedicarboxamide or pyridinedicarboxamide moieties and two 1,8-naphthyridine units linked by a crown ether like chain, have been synthesized and fully characterized by multinuclear NMR spectroscopy. X-ray diffraction analysis is provided for one of the macrocycles including a DMSO guest molecule. Binding constant determination of both hosts with four ureido derivatives, amongst them (+)-biotin methyl ester, was achieved by means of 1 H NMR titrations.
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关键词
Bisnaphthyridineamides,Benzenedicarboxamides,Pyridinedicarboxamides,Host–guest,Binding constants,MM calculations
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