Fe 3 O 4 nanoparticles as an efficient and reusable catalyst for the solvent-free synthesis of 9,9-dimethyl-9,10-dihydro-8 H -benzo-[ a ]xanthen-11(12 H )-ones
Chinese Journal of Catalysis(2015)
摘要
A simple and efficient method for the synthesis of 9,9-dimethyl-9,10-dihydro-8H-benzo-[α]xanthen-11(12)-one derivatives (DDBXs) was developed by the condensation reaction of various substituted aryl aldehydes with 2-naphthol and dimedone using Fe3O4 magnetic nanoparticles (MNPs) as a heterogeneous catalyst under solvent-free conditions at 90–110 °C. The experimental procedure is very simple, the products are formed in high yields and the catalyst is easily separated by applying an external magnetic field.
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关键词
Fe3O4 magnetic nano-particles,Three-component condensation,2-Naphthol,Dimedone,Xanthene
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