Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity

Nicolay Yu. Adonin,Sergey A. Prikhod’ko,Anton Yu. Shabalin,Igor P. Prosvirin,Vladimir I. Zaikovskii,Dmitry I. Kochubey,Dmitry A. Zyuzin,Valentin N. Parmon, Evgeny A. Monin, Irina A. Bykova, Petr O. Martynov,Sergey L. Rusakov,Pavel A. Storozhenko

Silicon（2015）

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摘要

A method for nanostructured cuprous chloride preparation by reductive thermolysis of a CuCl 2 ⋅2H 2 O and Cu(OH) 2 mixture in glycerol has been developed. The resultant CuCl was characterized with infrared spectroscopy, X-ray photoelectron spectroscopy, EXAFS spectroscopy, X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The prepared samples of CuCl demonstrated high catalytic activity in the “direct synthesis” of triethoxysilane.

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关键词

Direct synthesis,Silicon,Triethoxysilane,Trialkoxysilanes,Copper catalyst,Cuprous chloride,Nanostructured,Nanoparticles

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