Alternative Synthesis of A C,C-Diacetylenic Phosphaalkene

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS（2013）

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摘要

Bis(trimethylsilyl)-terminated C,C-diacetylenic phosphaalkene was prepared from Mes*PCl2 and a propargylic Grignard reagent that in turn was formed from 3-bromo-1,5-bis(trimethylsilyl)penta-1,4-diyne and Rieke-Mg.

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关键词

Phosphaalkene,alkyne,-conjugation,Rieke magnesium

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