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Flow and mixing efficiency characterisation in a CO 2 -assisted single-screw extrusion process by residence time distribution using Raman spectroscopy

Chemical Engineering Research and Design(2014)

Cited 9|Views4
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Abstract
•Polyamide foaming with adjustable porosity is achieved by extrusion assisted by CO2.•CO2 introduction has no effect on the flow pattern through the extruder.•In-line Raman spectroscopy was implemented on this process.•Residence time distribution can be accessed by this method.•Static mixer enhances the quantity of CO2 injected and improves the extrudates homogeneity.
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Key words
Hot-melt extrusion,Supercritical carbon dioxide,Residence time distribution,Static mixer,Raman spectroscopy
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