Synthesis and molecular structures of phenylacetylide triosmium clusters

Ol Ga A Kizas,Ekaterina A Ivanova,Ivan A Godovikov,Fedor M Dolgushin

Inorganica Chimica Acta（2011）

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摘要

The thermal decarbonylation of [Os3H(CO)10(μ,η2-CCPh)] (1) results in the complex [Os3H(CO)9(μ3,η2-CCPh)] (2) in a quantitative yield. The X-ray structural analysis has been performed for 1 and 2. The dependence of dynamic behavior of triosmium clusters on their structure is discussed.

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关键词

Triosmium clusters,X-ray analysis,Acetylenide ligand,Stereochemical non-rigidity

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