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FIRST TOTAL SYNTHESIS OF (+/-)-MYLTAYL-4(12)-ENE AND SINGLE-CRYSTAL X-RAY STRUCTURE OF EXO-12-NORMYLTAYLAN-4-YL 4-NITROBENZOATE

A SRIKRISHNA,CV YELAMAGGAD,K KRISHNAN,M NETHAJI

Journal of The Chemical Society, Chemical Communications（1994）

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Abstract
The total synthesis of the unusual sesquiterpene (+/-)-myltayl-4(12)-ene 3 starting from the readily available cyclogeraniol 5 and the single-crystal X-ray structure of the 4-nitrobenzoate 12 of the noralcohol 11 are described.
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single crystal,total synthesis
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