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Gold-Catalyzed Tandem Cycloisomerization-Halogenation of Chiral Homopropargyl Sulfonamides.

Chao Shu,Long Li,Cang-Hai Shen,Peng-Peng Ruan,Chao-Yue Liu,Long-Wu Ye

CHEMISTRY-A EUROPEAN JOURNAL（2016）

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Abstract
Two new gold-catalyzed tandem cycloisomerization-halogenation reactions of chiral homopropargyl sulfonamides have been developed. Various enantioenriched 3,3-diiodopyrrolidin-2-ols and 3-fluoropyrrolidin-2-ols were obtained in moderate-to-good yields with excellent enantio- and diastereoselectivity.
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Key words
cycloisomerization,gold,halogenation,heterocycles,homogeneous catalysis
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