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罗布麻叶黄酮类成分的UPLC-Q-TOF-MS分析

Jian-ping SONG,Hu XU,Fei CHEN,Xun-hong LIU,Feng-su ZHANG,Ya HOU,Yang MA

Zhong yao cai = Zhongyaocai = Journal of Chinese medicinal materials（2014）

Cited 2|Views21
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Abstract
目的:建立超高效液相色谱-四极杆飞行时间质谱(UPLC-Q-TOF-MS)对罗布麻叶中黄酮类成分分析的方法.方法:采用Alltima C18色谱柱(250 mm×4.6 mm,5μm),以乙腈-1％醋酸为流动相,梯度洗脱,流速为0.8mL/min,检测波长为254 nm,柱温为30℃.在电喷雾负离子模式下监测采集数据.结果:初步鉴定出11个黄酮类化合物,并同时测定其中6个黄酮的含量.6个黄酮的浓度与峰面积的线性关系良好(r＞0.9996),加样回收率为94.3％ ～ 103.3％.结论:该方法准确可靠,重现性好,可作为罗布麻叶内在质量评价的依据.
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Key words
UPLC-Q-TOF-MS,Apocynum venetom L.leaves,Flavonoids
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