IRMS detection of testosterone manipulated with 13C labeled standards in human urine by removing the labeled 13C.

Jingzhu Wang,Rui Yang,Wenning Yang,Xin Liu,Yanyi Xing,Youxuan Xu

Analytica Chimica Acta（2014）

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摘要

•13C labeled testosterone can be used to adjust the isotope ratio of testosterone.•The novel testosterone cannot be detected by the regular IRMS method in doping test.•A method was explored to remove the labeled 13C.•The established method can be used to detect the manipulated testosterone.

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关键词

Manipulated testosterone,13C labeled standard,Doping control,Isotope ratio mass spectrometry

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