Controllable fabrication of δ-MnO2 microspheres and α-MnO2 nanorods
MATERIALS AND DESIGN, PTS 1-3(2011)
Abstract
MnO2 nanostructure was synthesized via a redox reaction of potassium permanganate in hydrochloric acid solution below 100 degrees C at open environment. The effects of pH value in solution and reaction temperature on the crystal structure and morphology of MnO2 were investigated. It was revealed that layer folded delta-MnO2 microspheres were obtained at low reaction temperature and low HCl concentration, whereas alpha-MnO2 single-crystal nanorods were fabricated with increasing reaction temperature and HCl concentration. The possible formation mechanism of delta-MnO2 microspheres and alpha-MnO2 nanorods is suggested.
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Key words
Nanostructured materials,X-ray diffraction,MnO2
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