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调节pH抑制亚硝酸盐对碘量法测定溶解氧干扰的抑制作用

Xiandai Huagong/Modern Chemical Industry(2011)

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Abstract
为进一步提高碘量法测定溶解氧(DO)对亚硝酸盐存在的上限,提出在滴定前调节溶液pH在4~5,以抑制亚硝酸盐的干扰.实验表明此法适用于亚硝酸盐质量浓度在5~300 mg/L的水样溶解氧测定,在较高浓度亚硝酸盐存在的条件下,此法对DO质量浓度在2~10 mg/L的水样均具有较高的准确度.
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Key words
Dissolved oxygen,Iodometry,Nitrite,pH
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