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微波法合成含二茂铁基查尔酮

Yuting Liu,Huixin Yan,Dawei Yin,Donglin Miao

Speciality Petrochemicals（2010）

Cited 5|Views3
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Abstract
实验以微波法合成一种含二茂铁基查尔酮.讨论了催化剂、反应物料摩尔比、反应时间、微波辐射功率等对产率的影响.实验结果表明,微波法合成二茂铁基查尔酮的最佳条件为:催化剂为KF/Al2O3,n(乙酰基二茂铁)∶n(苯甲醛)=1∶1.2,反应时间为4 min,微波辐射功率为140 W.微波法合成二茂铁基查尔酮的产率达86.7%.目标产物结构经IR,1H NMR 进行了验证.
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Key words
Acetylferrocene,Chaicones,Microwave irradiation
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