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Synthesis Of [3-H-3]20(S)-Protopanaxadiol

Jian Meng,Lizhi Zhao,Youhong Hu,Xiaoyan Chen,Dafang Zhong

JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS（2009）

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Abstract
[3-H-3]20(S)-Protopanaxadiol (PPD) was prepared via selective reduction of PPD dioxide with sodium borotritide in N,N-dimethyl acetamide. A radiochemical yield of 22% was obtained. The radiochemical purity of the final product was 99% and the ratio of C-3/C-12 tritium labeling was 97:3.
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20(S)-protopanaxadiol, regioselective tritium-reductions of carbonyl functions, radiosynthesis
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