New synthesis of (+/-)shikalkin

Chinese Chemical Letters(2002)

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摘要
The new synthetic route of (+/-)shikalkin 1 was developed. 3-(1-Hydroxy-4-methyl-3-pentenyl)-5, 8-dimethoxy-1-naphthol 8 was obtained from compound 3 in 10 steps. Then (+/-)shikalkin I was synthesized from 8 in one step with reagents AgO/HNO3 in 1, 4-dioxane.
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关键词
shikalkin,synthesis
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