A short and highly stereoselective synthesis of cerebrosterol
CHINESE JOURNAL OF CHEMISTRY（2002）
Abstract
The title compound, cerebrosterol, has been synthesized in five steps with 61.5% overall yield and > 99.9% de from 3alpha, 6alpha-dimethoxymethoxyl-5p-cholane-24-al as a key intermediate, which was prepared from methyl 3alpha,6alpha-dibydroxy hyodeoxy-cholanate.
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Key words
cerebrosterol,methyl 3 alpha, 6 alpha-dihydroxy hyodeoxycholanate,diisopropylzinc,stereoselective synthesis
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