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Synthesis and Properties of Sodium Mono-Alkylamide Phthalate Surfactants

Journal of Surfactants and Detergents(2012)

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Abstract
The synthesis of a series of sodium mono-alkylamide phthalate surfactants is described, and the surface activity properties of the surfactants are reported. The mono-alkylamide phthalic acids were synthesized by amidation using primary aliphatic amines (lauryl, myristyl, cetyl) and phthalic anhydride as starting material. They were structurally characterized by IR, 1 H NMR and MS. The sodium mono-alkylamide phthalate surfactants were prepared by neutralization of the precursor acids with sodium hydroxide. They reduced the surface tension of water to 30–38 mN m −1 at concentration levels of 10 −4 mol L −1 .
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Key words
Phthalate,Alkylamide,Synthesis,Characterization
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