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Total synthesis of (±)-pallambins C and D.

Xue-Song Xu,Zhen-Wu Li,Yi-Jun Zhang,Xiao-Shui Peng,Henry N C Wong

CHEMICAL COMMUNICATIONS（2012）

Cited 29|Views6
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Abstract
The first total synthesis of (+/-)-pallambins C and D has been accomplished in a linear 38 step reaction from (+/-)-Wieland-Miescher ketone. The key conversions are featured as follows: a Grob fragmentation-intramolecular aldol cyclization and a thiourea/palladium-catalyzed carbonylative annulation.
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