A low temperature route to prepare LaFeO3 and LaCoO3
Materials Letters(2007)
摘要
A combination of digestion and further low temperature calcination to crystallize the product was employed to prepare LaFeO3 (LF) and LaCoO3 (LC) powders. Freshly co-precipitated lanthanum and ferric (or cobalt) hydroxide gels by sodium hydroxide were allowed to react at 100 °C under refluxing and stirring conditions for 4–6 h. These oven dried powders were heated at 450 °C to form crystalline LF (or LC) powders. The phase contents and lattice parameters were investigated by X-ray diffraction (XRD). Transmission electron microscope (TEM) investigations were carried out to examine the morphology and average particle size of these powders.
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关键词
Chemical synthesis,X-ray diffraction,Transmission electron microscopy,Precipitation,LaFeO3
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