微波辐射下5,7-二硝基-8-羟基喹啉的合成
Chemical Reagents（2007）
Abstract
在微波辐射下,8-羟基喹啉与硝酸铈铵在乙腈和聚乙二醇溶液中反应生成5,7-二硝基-8-羟基喹啉.最佳反应条件勾n(8-羟基喹啉)∶n(硝酸铈铵)=1∶1.3,反应时间6 min,5,7-二硝基-8-羟基喹啉的产率达76.2%.
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Key words
nitration,5,8-hydroxyquinoline,7-dinitro-8-hydroxyquinoline,cerium ammonium nitrate
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