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Preparation of 3-amino-1,4-benzodiazepin-2-ones via direct azidation with trisyl azide

John W. Butcher,Nigel J. Liverton,Harold G. Selnick,Jason M. Elliot,Garry R. Smith,Andrew J. Tebben,David A. Pribush,John S. Wai,David A. Claremon

TETRAHEDRON LETTERS（1996）

Cited 19|Views40
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Abstract
An efficient synthesis of 3-amino-1,4-benzodiazepin-2-ones utilizing triisopropylbenzenesulfonyl azide (trisyl azide) for the direct azidation of 1,4-benzodiazepin-2-ones is described. Copyright (C) 1996 Elsevier Science Ltd
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trisyl azide,direct azidation
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