N,N′-双(邻菲啰啉-2-甲酰基)-4,4′-二氨基苯基甲烷的合成
Chemical Reagents(2008)
Abstract
以邻菲啰啉为起始原料,与双氧水反应合成邻菲啰啉-N-氧化物,接着与苯甲酰氯、氰化钾、NaOH水溶液一一反应合成中间体邻菲啰啉-2-甲酸,再与4,4′-二氨基苯基甲烷进行酰胺化反应合成目标产物。其结构通过红外光谱、元素分析、核磁共振谱和质谱进行了表征。
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Key words
1,synthesis,amidation,10-phenanthroline
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