Radical alkylation of N-alkyl 1,2,4-triazoles

Karl B Hansen,Shawn A Springfield,Richard Desmond,Paul N Devine,Edward J.J Grabowski,Paul J Reider

Tetrahedron Letters（2001）

引用 17|浏览17

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摘要

Reaction of 1-N-alkyl triazoles with an alkyl radical generated from the corresponding carboxylic acid, affords the triazole ring alkylated selectively in the 5 position. Secondary radicals perform best in the intermolecular reaction, while primary radicals alkylate the triazole in an intramolecular fashion.

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