Ruthenium carbonyl clusters containing PMe2(nap) and derived ligands (nap=1-naphthyl): generation of naphthalyne derivatives

Michael I. Bruce,Paul A. Humphrey,Reinhard Schmutzler,Brian W. Skelton,Allan H. White

Journal of Organometallic Chemistry（2005）

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摘要

Reactions of 1,8-(PMe2)2C10H8 with Ru3(CO)12 or Ru3(μ-dppm)(CO)10 results in ready replacement of one PMe2 group by H to give Ru3(μ-dppm)a(CO)11-2a{PMe2(nap)}; thermolysis affords clusters containing μ3-naphthalyne groups.

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