叔胺类化合物的合成新方法
Journal of China West Normal University(Natural Sciences)(2007)
Abstract
提出了一种由仲胺合成叔胺的新方法.仲胺与丙烯腈的Michael加成产物与卤代烃发生季铵化,生成的季铵盐完成Hoffmann型消除反应,合成了系列叔胺类化合物3a,3b,6,其结构经IR,1HNMR,MS谱证实.本文还就反应温度、溶剂、反应物结构等对反应的影响做了详细探讨,确定了最佳反应条件.
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Key words
Quanternization,tertiaryamines,Hoffmann elimination,Michael addition,synthesis
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