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L-苯甘氨酸衍生物新型三齿手性氨基醇的合成

LIU Feng-liang,XIAO Qing-bo,SHEN Xia,LIU Yan-ping,LIU Chang,YIN Jun

Guangzhou Chemistry（2011）

Cited 2|Views36
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Abstract
对叔丁基苯胺经二甲基化、甲酰化得到5-叔丁基-2-二甲氨基苯甲醛;L-苯甘氨酸经LiAlH4直接还原,得到的二齿手性氨基醇与上述醛经缩合、还原,得到新型三齿手性氨基醇(2S)-2-[(5-叔丁基-2-二甲氨基)苯基]甲氨基-2-苯基乙醇。用红外光谱(IR)、质谱(MS)和核磁共振氢谱(1H-NMR)等对产物进行了结构表征。
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Key words
L-phenyl glycine,4-tert-butyl aniline,polydentate chiral amino alcohol,LiAlH4
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