合成2,3,4,6-O-四苄基-α-D-葡萄糖三氯乙酰亚胺酯的工艺改进
Chinese Journal of Synthetic Chemistry（2013）
Abstract
以D-葡萄糖为起始原料,经甲基化、苄基保护和水解,再与三氯乙腈反应合成了2,3,4,6-O-四苄基-α-D-葡萄糖三氯乙酰亚胺酯,总收率44.2%,其结构经1H NMR和ESI-MS确证。
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Key words
D-glucose,trichloroacetimitate,process improvement,synthesis
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