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Facile Syntheses of AM-toxins and Analogs as Cyclic Depsipeptides by the Solid-phase Method.

Masahiro MIYASHITA,Tomoko NAKAMORI,Takahiro MURAI,Hisashi MIYAGAWA,Miki AKAMATSU,Tamio UENO

BIOSCIENCE BIOTECHNOLOGY AND BIOCHEMISTRY（2014）

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Abstract
The cyclic depsipeptides, AM-toxins I and II and AM-toxin I analogs, were efficiently and rapidly prepared by the Fmoc-based solid-phase method for the synthesis of linear depsipeptides, with N-[(dimethylamino)-1H-1,2,3-triazolo[4,5-b]pyridin-1-ylmethylene]-N-methylmethanaminium hexafluorophosphate N-oxide (HATU) being used for their subsequent cyclization.
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Key words
AM-toxin,host-specific toxin,cyclic depsipeptide,solid-phase synthesis,HATU
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