A one-step oxidative synthesis of trimethylantimony(v) diacylates

V. A. Dodonov,A. V. Gushchin,O. G. Vorob'ev,T. I. Zinov'eva

Russian Chemical Bulletin（1994）

Cited 4|Views6

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Abstract

Trimethylantimony(v) diacylates Me3Sb(OCOR)2 (R = H, Me, Ph) have been obtained in 72–75 % yield by the interaction of trimethylantimony withtert-butylhydroperoxide and carboxylic acids at the ratio of 1 : 1 : 2 in benzene (20 °C, 20 h) in the presence of sodium sulfate.

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Key words

trimethylantimony(v) diacylates, synthesis, trimethylantimony, oxidative acylation

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