肾上腺素电化学氧化生成肾上腺素红反应机理的薄层光谱电化学研究
Chemical Research(2010)
Abstract
应用长光程薄层电解池(石墨电极和铂片电极),使用循环伏安法(CV)和单电位阶跃计时吸收法(SPS/CA),研究了肾上腺在pH=2.5~7.0的McIlvaine缓冲溶液中电氧化生成肾上腺素红的反应机理,测定了表观速率常数kobs.结果表明:溶液pH值对肾上腺素的电氧化反应有很大影响,肾上腺素生成肾上腺素红的kobs随溶液pH值的增加而增大.
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Key words
electrochemical oxidation,reaction mechanism,adrenaline,adrenochrome,thin layer spectrum,electrochemistry
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