Preparation and dehydration behaviour of thomsonite with ideal chemical composition
Journal of Thermal Analysis(2014)
摘要
Thomsonite with ideal chemical composition and with an ordered framework structure was synthesised hydrothermally from zeolite Na−A, which was ground to X-ray amorphous, with 0.05 mol dm−3 CaCl2 solution at 200°C. The dehydration behaviour of the prepared thomsonite was examined by TG-DTA. It was revealed that thomsonite lost most of zeolitic water below 450°C in three steps at about 180°, 340° and 390°C. The peak profiles of, the two higher-temperature endotherms were sharp and similar, and the weight loss at each step was approximately equal.
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关键词
dehydration and preparation of thomsonite, 29Si and27Al NMR, TG-DTA
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