二胺型腰果酚基苯并嗪的合成工艺
Chemical Industry and Engineering Progress(2012)
Abstract
以己二胺、多聚甲醛和腰果酚为原料合成了一种二胺型腰果酚基苯并嗪单体.使用FTIR和1 H NMR对单体进行了化学结构表征.以产品收率为指标,考察了反应时间、反应温度、溶剂种类等反应条件对反应产物收率的影响,确定较佳反应条件为:反应时间5h,反应温度105℃,溶剂为甲苯。
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Key words
benzoxazine,hexamethylene diamine,characterization,synthesis
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