The carbonylation of methylacetate to acetic anhydride catalysed by [Cp∗Rh(CO)2] in the absence of hydrogen

Andrew C. Marr,Philip Lightfoot,Evert J. Ditzel,Andrew D. Poole,Gary P. Schwarz,Douglas F. Foster,David J. Cole-Hamilton

Inorganic Chemistry Communications（2000）

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摘要

[Cp∗Rh(CO)2] catalyses the carbonylation of methylacetate to acetic anhydride at 6.9 moldm3h−1 in the absence of hydrogen; [Cp∗RhI2(CO)] which forms from it is also catalytically active giving rates of 1.2 moldm3h−1 under the same conditions.

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关键词

Methyl acetate,Carbonylation,Acetic anhydride,Rhodium,Pentamethylcyclopentadienyl,WGSR

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