电解氢化物发生原子荧光法测定镉
Chinese Journal of Analysis Laboratory(2012)
Abstract
通过电解氢化物发生技术结合原子荧光光谱仪,采用自行设计的管式电解池,研究了管状阴极材料以及电解质种类、电解条件等因素对Cd的电解还原氢化物发生情况的影响。方法检出限为0.26μg/L,相对标准偏差为3.3%(n=11)。对标准物质海带及几种海产品中的Cd进行了测定,回收率在93%~110%之间。
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Key words
Atomic fluorescence spectrometry,Cd,Electrolytic hydride generation,Tubular cell
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