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高纯度单甘油月桂酸酯的合成

Henan Science(2013)

Cited 52|Views10
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Abstract
以非均相固体碱为催化剂,以月桂酸甲酯和1,2-O-异亚丙基甘油(简称保护甘油)为原料制备单甘油月桂酸酯,最佳反应条件为:原料比(月桂酸甲酯∶保护甘油,物质的量比)为1∶2.5,反应时间7 h,最佳反应温度为160℃,催化剂用量8%(占月桂酸甲酯质量百分比),在最佳条件下,取得了94.1%的产率.
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Key words
inhomogeneous solid alkali,high purity,synthesis of glycerol monostearate
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